Chromatographic Analysis of Pharmaceuticals

0.01 M ammonium acetic acid Acidified adjusted ammonium hydroxide Ammonium hydroxide methanol Anal analysis analytical application approach assay automated buffer Bulk HPLC Silica Bulk TLC Dissolve capillary Capsules centrifuge Chem chiral chloro chloroform Chromatogr column Compound Formulation Mode containing Convention Cream derivatization Detection Comments Reference detector determination diethylamine Dilute Dissolve in methanol drugs enantiomers extract filter Formulation Mode Sample gas chromatography heat identification inate Injection iodoplat ISTD liquid chromatography methanol Silica methanolic potassium hydroxide method Mobile Phase Detection Mode Sample Pretreatment nm USP XXI Pharm pharmaceutical Phase Detection Comments phosphate powder preparation Pretreatment Sorbent Temp procedure purity Quantitative reagents Reference resolution robotic Sample Pretreatment Sorbent selectivity separation Shake Silica Methylene chloride sodium solution solvent stability standard stationary phase sulfate Table Tablets Tablets HPLC technique tion United States Pharmacopeial various volume